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Submitted
May 29, 2018
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May 29, 2018
Published
May 29, 2018
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Abstract

[SYNTHESIS AND CHARACTERIZATION OF XEROGEL RESULTS OF COPRECIPITATION OF LONG BEACH BENGKULU BEACH].  This research aims to synthesize and characterization to  Xerogel which synthesizes from Pantai Panjang  sands Bengkulu. The method used for this study to synthesizes Xerogel is to use the coprecipitation method. Qualitative XRF test against raw sand  materials that were used show that the content of the element is the most significant element of Si. The first  stages of the synthesis of Xerogel is a purification of the sand sample..  Xerogel synthesis is carried out in two phases, namely the manufacture of aqueous solutions of Sodium Silicate and continued with the formation of a gel. The production of Sodium Silicate solution is done using the NaOH concentration at 5, 6 and 7 M.  Gel formation process is done by adding a solution of HCl 10 M into the solution of Sodium Silicate, followed by process of filtration, washing and drying in the oven. The results showed that the optimum conditions of synthesis of Xerogel   obtained  using 6 M NaOH  , with a yield obtained is amounting at 0.8%. The results of the test by XRD shows that the silica crystal structure  on Xerogel  are amorphous-shaped. SEM-EDS test results show that the acquired  Xerogel on research has a smooth texture and size is not homogeneous with the highest content of elements are the elements Si and O.  PSA test shows that particle size in Xerogel an average at 191.4 nm. 

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How to Cite
Meyori, F., Elvia, R., & Candra, I. N. (2018). SINTESIS DAN KARAKTERISASI XEROGEL HASIL KOPRESIPITASI DARI PASIR PANTAI PANJANG BENGKULU. ALOTROP, 2(1). https://doi.org/10.33369/atp.v2i1.4646
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References

  1. Elvia, R., A. H. Cahyana, W. Wibowo., Catalytic Acetylation of (+)- Cedrol with Heterogeneous Catalyst H2SO4/SiO2 under Solvent freeConditions.Chemistry International, 2015:1(4) :196-201.
  2. Kristiyanti, Istofa, Beny Syawaludin, Karakterisasi Kaca Timbal Untuk Pe-lindung Penangkap Citra Sinar –X, Prima, 2012: 9(2): 86-93.
  3. Nuryono , Narsito, Pengaruh Konsentrasi Asam Terhadap Karakter Silika Gel Hasil Sintesis dari Natrium Silikat, Indo. J. Chem., 2005:5(1):23 – 30.
  4. Madina, F.E., Rina Elvia., I Nyoman Chandra., Analisis Kapasitas Adsorpsi Silika dari Pasir Pantai Panjang Bengkulu Terhadap Pewarna Rhodamine B. Alotrop , 2017,1(2):98-101.
  5. Febriyanti, R., Titin Anita Zaharah , Nelly Wahyuni, Optimasi Waktu Kontak Modifikasi Silika Gel Dari Limbah Kaca Menggunakan Tributilamina, JKK, 2014: 3(3):25-29.
  6. Ngatijo, F. Faried, I. Lestari. Pemanfa-atan Abu Sekam Padi (ASP) Payo dari Kerinci sebagai Sumber Silika dan Apli-kasinya dalam Ekstraksi Fasa Padat Ion Tembaga (II). Jurnal Penelitian Universitas Jambi Seri Sains, 2011:13(2):47-52.
  7. Yusuf, M., D. Suhendar, E. P. Hadisantoso., Studi Karakterisasi Silika Gel Hasil Sintesis dari Abu Ampas Tebu dengan Variasi Konsentrasi Asam Klo-rida. Jurnal Istek, 2014: 8(1):16-28.
  8. Eka Suprihatin, Titin Anita Zaharah, Nelly Wahyuni, Pembuatan Membran Si-lika dari Ply Ash dan Aplikasinya Untuk Menurunkan Kadar COD Dan BOD Limbah Cair Kelapa Sawit, JKK, 2015:4(3): 48-53.
  9. Pertama , I.S., Titin Anita Zahara , Nelly Wahyuni, Optimasi Waktu dan Suhu Pengeringan Modifikasi Silika Gel Berbahan Dasar Abu Sekam Padi dengan Tri-butilamina, JKK, 2014: 3(4):39-45.
  10. Handayani, P.A., Eko Nurjanah, Wara Dyah Pita Rengga, Pemanfaatan Limbah Sekam Padi Menjadi Silika Gel, Jurnal Bahan Alam Terbarukan, 2015:4(2):55-59.
  11. Hayati, R., Astuti., Sintesis Nanopartikel Silika dari Pasir Pantai Purus Padang Sumatera Barat dengan Metode Kopresipitasi. Jurnal Fisika Unand., 2015:4(3): 282-287.
  12. Hadi, S.M., Triwikantoro, M. Zainuri, Darminto., Pengaruh Molaritas NaOH pada Sintesis Nanosilika Berbasis Pasir Bancar Tuban. Jurnal Penelitian Fisika dan Aplikasinya, 2013:3(2) :12-17.
  13. Hadi, S,M,, Triwikantoro., Sintesis Silika Berbasis Pasir Alam Bancar menggu-nakan Metode Kopresipitasi. Jurnal Fisika dan Aplikasinya, 2011:7(2):1-4.
  14. Adjiantoro, B., Efendi Mabruri, Pengaruh Waktu Pelindian Pada Proses Pemurnian Silikon Tingkat Metalurgi Menggunakan Larutan HCl, Majalah Metalurgi, 2012: 27(1):1-6.
  15. Trivana L., Sri Sugiarti; Eti Rohaeti, Sintesis dan Karakterisasi Natrium Silikat (Na2SiO3) Dari Sekam Padi, Jurnal Sains dan Teknologi Lingkungan, 2015:7(2): 66-75.
  16. Adziimaa, A.F., Doty Dewi Risanti, Lizda Johar Mawarni, Sintesis Natrium Silikat dari Lumpur Lapindo sebagai Inhibitor Korosi, Jurnal Teknik Pomits, 2013:2(2): F-384-F-389.
  17. Mujiyanti, D.R., Nuryono, Eko Sri Kunarti, Sintesis dan Karakterisasi Silika Gel Dari Abu Sekam Padi yang Dimobilisasi Dengan 3-(Trimetoksisilil)-1-Propantiol, Sains dan Terapan Kimia, 2010: 4(2):150-167.
  18. Meirawati, D., S. Wardhani, R. T. Tjahjanto., Studi Pengaruh Konsentrasi HCl dan Waktu Aging (Pematangan Gel) terhadap Sintesis Silika Xerogel Berba-han Dasar Pasir Kuarsa Bangka. Kimia Student Journal, 2013:2(2):524-531.
  19. Saputra DS, R.M., Rudiyansyah , Nelly Wahyuni,Sintesis dan Karakterisasi Silika Gel Dari Limbah Kaca Termodifikasi Asam Stearat, JKK, 2014 : 3(3):36-42.
  20. Ayu , A.M., Sri Wardhani, Darjito, Studi Pengaruh Konsentrasi NaOH dan pH Terhadap Sintesis Silika Xerogel Berbahan Dasar Pasir Kuarsa, , Kimia Student Journal, 2013:2(2):517-523.
  21. Latif, C., Triwikantoro, Munasir, Pengaruh Variasi Temperatur Kalsinasi Pada Struktur Silika, Jurnal Sains Dan Seni Pomits , 2014:3(1): B-4- B-7.
  22. Munasir , Triwikantoro , Moch.Zainuri, Darminto., Ekstraksi Dan Sintesis Nanosilika Berbasis Pasir Bancar Dengan Metode Basah , Jurnal Penelitian Fisika dan Aplikasinya, 2013:3(2):12-17.
  23. Izzati, H. N., F. Nisak, Munasir., Sintesis dan Karakterisasi Kekristalan Nanosilika Berbasis Pasir Bancar. Jurnal Inovasi Fisika Indonesia, 2013:2(3):19-22.
  24. Iman P, T., Arneli , Ahmad Suseno , Pengaruh Konsentrasi NaOH Pada Pengambilan Silika Dari Abu Sekam Padi Untuk Sintesis Zeolit dan Aplikasi Sebagai Builder Deterjen, Chem Info , 2013: 1(1): 275–282.
  25. Dewi, A.Y.K., Sigit Priatmoko, Sri Wah-yun, Elektroda Solar Cell Berbasis Komposit TiO2/SiO2 Sebagai Energi Alternatif Terbarukan, Indo. J. Chem. Sci, 2012:1(2):92-97.