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Abstract
[ANALYSIS OF SILICA ADSORPTION CAPACITY FROM THE SAND OF PANTAI PANJANG BENGKULU AGAINST RHODAMINE B DYES ] This research was aimed to study the adsorption capacity of synthetic silica on Rhodamine B dyes. Synthetic silica was obtained from the sand of Pantai Panjang Bengkulu by alkali fusion method using KOH at 360 °C for 4 hours in furnace to obtain potassium silicate crystals (K2SiO3). The crystals were then added 500 mL aqua DM, stirred and sterilized for 24 hours folloed by filtered. The filtrate was dropped with 10 M HCl solution until the pH of filtrate solution reached at 1 to 2 and formed a silent white gel for 24 hours. Moreover, the gel was filtered with filter paper and washed with aqua DM until pH is neutral and free from KCl, and dried in an oven at 60 °C for 18 hours. The obtained silica powder is then smoothed with mortar and weighed. The adsorbent of Rhodamine B dyes using the synthetic silica powder was performed on pH variation at 2, 3, 4, 5, 6, and 7 , and variation of contact time at 10, 20, 30, 40, 50, and 60 min. The results showed that the optimum condition of adsorption of Rhodamine B by silica from Pantai Panjang sand occured at optimum pH 2 and optimum contact time 20 minutes; with adsorption capacity of 4.95 mg / g and 4.79 mg/g; and with adsorption efficiency of 99.00% and 95.89%.
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References
- Sumarlin, La Ode, Indentifikasi Pewarna Sintetis Pada Produk Pangan Yang Beredar di Jakarta dan Ciputat. Jurnal Kimia Valensi. 2010:1(6): 274-283.
- Puspita ,M, M. Lutfi Firdaus, Nurhamidah. Pemanfaatan Arang Aktif Sabut Kelapa Sawit Sebagai Adsorben Zat Warna Sintesis Reactive Red-120 dan Direct Green-26. Alotrop. 2017:1(1): 75-79.
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- Munasir, Triwikantoro, Mochamad Zainuri, Darminto. Uji XRD Dan XRF Pada Bahan Mineral (Batu dan Pasir) Sebagai Sumber Material Cerdas (CaCO3 dan SiO2). Jurnal Penelitian Fisika Dan Aplikasinya (JPFA). 2012: 2(1): 20-29.
- Darwis, D, Rany Khaeroni, Iqbal. Pemurnian dan Karakterisasi Silika Menggunakan Metode Purifikasi (Leaching) dengan Variasi Waktu Milling Pada Pasir Kuarsa Desa Pasir Putih Kecamatan Pamona Selatan Kabupaten Poso. Natural Science Journal of Science and Technology. 2017: 6(2): 187-193.
- Munasir, Triwikantoro, Mochamad Zainuri, Darminto , Ekstraksi Dan Sintesis Nanosilika Berbasis Pasir Bancar Dengan Metode Basah, Jurnal Penelitian Fisika dan Aplikasinya (JPFA). 2013: 3(2): 12-16.
- Arivoli, Shanmugam. 2009. Adsorption of Rhodamine B by Acid Active Carbon – Kinetic, Thermodynamic, and Equilibrium Studies. Orbital. 2009: (l) 2: 37-43.
- Gan, Pei dan Li, Sam Fong 2013. Efficient Removal of Rhodamine B Using a Rice Hull – Based Silika Supproted Iron Catalyst by Fenton-Like Process. Chemical Engineering Journal. 351 – 363.
- Rusdiarso, B, Eko Sri Kunarti, Saprini Hamdiani, Synthesis Of Mesoporous Methyl-Silica Hybrid For Adsorption Of Alizarin Red-S. Indo.J.Chem. 2008: 8(2):193-199
References
Sumarlin, La Ode, Indentifikasi Pewarna Sintetis Pada Produk Pangan Yang Beredar di Jakarta dan Ciputat. Jurnal Kimia Valensi. 2010:1(6): 274-283.
Puspita ,M, M. Lutfi Firdaus, Nurhamidah. Pemanfaatan Arang Aktif Sabut Kelapa Sawit Sebagai Adsorben Zat Warna Sintesis Reactive Red-120 dan Direct Green-26. Alotrop. 2017:1(1): 75-79.
Sari, R.A, M. Lutfi Firdaus, Rina Elvia, Penentuan Kesetimbangan Termodinamika dan Kinetika Adsorpsi Arang Aktif Tempurung Kelapa Sawit Pada Zat Warna Reactive Red. Alotrop. 2017: 1(1): 10-14.
Sutrisno, B, Arif Hidayat, Zahrul Mufrodi, Modifikasi Limbah Abu Layang Menjadi Adsorben Untuk Mengurangi Limbah Zat Warna Pada Industri Tekstil. Chemica. 2014: 1(2):57-66.
Munasir, Triwikantoro, Mochamad Zainuri, Darminto. Uji XRD Dan XRF Pada Bahan Mineral (Batu dan Pasir) Sebagai Sumber Material Cerdas (CaCO3 dan SiO2). Jurnal Penelitian Fisika Dan Aplikasinya (JPFA). 2012: 2(1): 20-29.
Darwis, D, Rany Khaeroni, Iqbal. Pemurnian dan Karakterisasi Silika Menggunakan Metode Purifikasi (Leaching) dengan Variasi Waktu Milling Pada Pasir Kuarsa Desa Pasir Putih Kecamatan Pamona Selatan Kabupaten Poso. Natural Science Journal of Science and Technology. 2017: 6(2): 187-193.
Munasir, Triwikantoro, Mochamad Zainuri, Darminto , Ekstraksi Dan Sintesis Nanosilika Berbasis Pasir Bancar Dengan Metode Basah, Jurnal Penelitian Fisika dan Aplikasinya (JPFA). 2013: 3(2): 12-16.
Arivoli, Shanmugam. 2009. Adsorption of Rhodamine B by Acid Active Carbon – Kinetic, Thermodynamic, and Equilibrium Studies. Orbital. 2009: (l) 2: 37-43.
Gan, Pei dan Li, Sam Fong 2013. Efficient Removal of Rhodamine B Using a Rice Hull – Based Silika Supproted Iron Catalyst by Fenton-Like Process. Chemical Engineering Journal. 351 – 363.
Rusdiarso, B, Eko Sri Kunarti, Saprini Hamdiani, Synthesis Of Mesoporous Methyl-Silica Hybrid For Adsorption Of Alizarin Red-S. Indo.J.Chem. 2008: 8(2):193-199